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Mazzaro, Raffaello
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Publications (5/5 displayed)
- 2023An advanced PdNPs@MoS<sub>2</sub> nanocomposite for efficient oxygen evolution reaction in alkaline mediacitations
- 2023Photoelectrochemical Valorization of Biomass Derivatives with Hematite Photoanodes Modified by Cocatalystscitations
- 2023Robust Molecular Anodes for Electrocatalytic Water Oxidation Based on Electropolymerized Molecular Cu Complexescitations
- 2022NiCo2O4 nanostructures loaded onto pencil graphite rod: An advanced composite material for oxygen evolution reactioncitations
- 2022NiNP@rGO Nanocomposites as Heterogeneous Catalysts for Thiocarboxylation Cross-Coupling Reactionscitations
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article
NiNP@rGO Nanocomposites as Heterogeneous Catalysts for Thiocarboxylation Cross-Coupling Reactions
Abstract
<jats:title>Abstract</jats:title><jats:p>A new type of ligand-free Ni-nanoparticles supported on rGO (size distribution average d = 9 ± 3 nm) was prepared and fully characterized via morphological (Fe-SEM), structural (P-XRD, HR-TEM), and spectroscopic (ICP-EOS, XPS) analysis tools. The metal composite was effectively employed in the unprecedented heterogeneously Ni-assisted cross-coupling reaction of aryl/vinyl iodides and thiocarboxylates. A range of sulfur-containing aryl as well as vinyl derivatives (15 examples) was achieved in high yields (up to 82%), under mild reaction conditions, and with wide functional group tolerance.</jats:p>