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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Arrighi, Valeria
Heriot-Watt University
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (16/16 displayed)
- 2024A Sacrificial Linker in Biodegradable Polyesters for Accelerated Photoinduced Degradation, Monitored by Continuous Atline SEC Analysis
- 2019The Effect of the Isomeric Chlorine Substitutions on the Honeycomb-Patterned Films of Poly(x-chlorostyrene)s/Polystyrene Blends and Copolymers via Static Breath Figure Techniquecitations
- 2018Efficient defluoridation of water by Monetite nanorodscitations
- 2015Microwave and thermal curing of an epoxy resin for microelectronic applicationscitations
- 2014Synthesis of Polystyrene Grafting Filler Nanoparticles
- 2014Physical Aging of Polymer Blendscitations
- 2008Interpolymer complexation in hydrolysed poly(styrene-co-maleic anhydride)/poly(styrene-co-4-vinylpyridine)citations
- 2008Interpolymer complexation and thermal behaviour of poly(styrene-co-maleic acid)/poly(vinyl pyrrolidone) mixturescitations
- 2007Miscibility study of stereoregular poly(methyl methacrylate) blends. Experimental determination of phase diagrams and predictionscitations
- 2006An improved algorithm for the fourier integral of the KWW function and its application to neutron scattering and dielectric datacitations
- 2004Dielectric relaxations in poly(di-n-alkyl itaconate)scitations
- 2004Order in amorphous di-n-alkyl itaconate polymers, copolymers, and blendscitations
- 2003Effects of Tacticity on the Local Dynamics of Polypropylene Meltscitations
- 2002Phase behaviour of SMMA and SAN blends using Flory's equation of state theorycitations
- 2001Lyotropic liquid crystalline cellulose derivatives in blends and molecular composites
- 2000Observation of Local Order in Poly(di-n-alkyl itaconate)scitations
Places of action
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article
Microwave and thermal curing of an epoxy resin for microelectronic applications
Abstract
<p>Microwave curing of thermosetting polymers has a number of advantages to natural or thermal oven curing and is considered a cost-effective alternative. Here we present a detailed study of a commercially available epoxy resin, EO1080. Samples that are thermally cured are compared to curing using a recently developed modular microwave processing system. For commercial purposes it is crucial to demonstrate that microwave curing does not adversely affect the thermal and chemical properties of the material. Therefore, the kinetics of cure and various post cure properties of the resin are investigated. Attenuated Total Reflectance Fourier-Transform Infrared (ATR-FTIR) analysis shows no significant difference between the conventionally and microwave cured samples. Differential scanning calorimetry (DSC) is used to monitor the kinetics of the curing reaction, as well as determine the thermal and ageing properties of the material. As expected, the rate of curing is higher when using microwave energy and we attempt to quantify differences compared to conventional thermal curing. No change in glass transition temperature (T<inf>g</inf>) is observed. For the first time, enthalpy relaxation measurements performed on conventional and microwave cured samples are reported and these indicate similar ageing properties at any given temperature under T<inf>g</inf>.</p>