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Kainzbauer, Peter
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article
The Ternary Bi-Mn-Sb Phase Diagram and the Crystal Structure of the Ternary Τ Phase Bi0.8MnSb0.2
Abstract
<p>The phase equilibria of the ternary system Bi-Mn-Sb were experimentally investigated with focus on the possible existence of a ferromagnetic continuous solid solution between α-BiMn and MnSb at 320 °C (both B8<sub>1</sub>, NiAs structure type). Isothermal sections at 320 and 600 °C were studied applying powder x-ray diffraction and scanning electron microscopy including energy dispersive x-ray spectroscopy. The corresponding isothermal sections at 320 and 600 °C were established based on these results. A complete ternary reaction scheme (Scheil diagram) and a liquidus surface projection based on primary crystallization analyses and DTA (differential thermal analysis) were constructed. Furthermore, the vertical section at 10 at.% Sb was studied by DTA. A continuous solid solution between the isostructural phases α-BiMn and MnSb, as reported in the literature, could not be confirmed. A new hexagonal P6<sub>3</sub>/mmc setting of the known orthorhombic P222<sub>1</sub>ternary phase Bi<sub>x</sub>MnSb<sub>1−x</sub>, based on single-crystal x-ray diffraction data, is described.</p>