| People | Locations | Statistics |
|---|---|---|
| Naji, M. |
| |
| Motta, Antonella |
| |
| Aletan, Dirar |
| |
| Mohamed, Tarek |
| |
| Ertürk, Emre |
| |
| Taccardi, Nicola |
| |
| Kononenko, Denys |
| |
| Petrov, R. H. | Madrid |
|
| Alshaaer, Mazen | Brussels |
|
| Bih, L. |
| |
| Casati, R. |
| |
| Muller, Hermance |
| |
| Kočí, Jan | Prague |
|
| Šuljagić, Marija |
| |
| Kalteremidou, Kalliopi-Artemi | Brussels |
|
| Azam, Siraj |
| |
| Ospanova, Alyiya |
| |
| Blanpain, Bart |
| |
| Ali, M. A. |
| |
| Popa, V. |
| |
| Rančić, M. |
| |
| Ollier, Nadège |
| |
| Azevedo, Nuno Monteiro |
| |
| Landes, Michael |
| |
| Rignanese, Gian-Marco |
|
Haddad, Paul
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (7/7 displayed)
- 2018Evaluation of a cooling/heating-assisted microextraction instrument using a needle trap device packed with aminosilica/graphene oxide nanocomposites, covalently attached to cottoncitations
- 2018Synthesis and characterization of MIL-101(Cr) intercalated by polyaniline composite, doped with silica nanoparticles and its evaluation as an efficient solid-phase extraction sorbentcitations
- 2016Open tubular-capillary electrochromatography: developments and applications from 2013 to 2015citations
- 2010Photolithographic patterning of conducting polyaniline films via flash weldingcitations
- 2010Cyano bonded silica monolith - development of an in situ modification method for analytical scale columnscitations
- 2009Profiling the chemical composition of explosives
- 2001New isoelectric buffers for capillary electrophoresis: N-carboxymethylated polyethyleneimine as a macromolecular isoelectric buffercitations
Places of action
| Organizations | Location | People |
|---|
article
Synthesis and characterization of MIL-101(Cr) intercalated by polyaniline composite, doped with silica nanoparticles and its evaluation as an efficient solid-phase extraction sorbent
Abstract
A metal?organic framework/polyaniline composite was synthesized and doped with silica nanoparticles. The structure and morphology of the composite were characterized using Fourier transform infrared spectroscopy and scanning electron microscopy. It was packed inside a cartridge and evaluated for the solid‐phase extraction of thymol and carvacrol, followed by gas chromatography with flame ionization detection measurement. The influence of the important experimental variables on the efficiency of the proposed method, including pH, ionic strength, volume of sample solution and type, and volume of eluent were studied and optimized. Under the optimal conditions, the relative standard deviations were found to be 3.8 and 9.8% for thymol and carvacrol, respectively, and the corresponding limits of detection were 0.1 and 1.0 ng/mL. The linear dynamic ranges for the calibration curves of the analytes were 10?10000 ng/mL, with determination coefficients (<i>R</i><sup>2</sup>) > 0.993. The limits of quantifications were found to be 0.01 and 0.5 μg/mL, for thymol and carvacrol, respectively. The prepared nanocomposite sorbent was applied successfully to the extraction and determination of thymol and carvacrol in <i>Lamiaceae</i> plant extracts and a honey sample, with relative recoveries in the range of 90.28?122.0%.