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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Schwaiger, Ruth
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (25/25 displayed)
- 2024Enabling High-Performance Hybrid Solid-State Batteries by Improving the Microstructure of Free-Standing LATP/LFP Composite Cathodes
- 2024Controlling shear band instability by nanoscale heterogeneities in metallic nanoglasses
- 2024Microstructure Characterization and Mechanical Properties of Polymer‐Derived (HfₓTa₁₋ₓ)C/SiC Ceramic Prepared upon Field‐Assisted Sintering Technique/Spark Plasma Sintering
- 2024Enabling High-Performance Hybrid Solid-State Batteries by Improving the Microstructure of Free-Standing LATP/LFP Composite Cathodes.citations
- 2024Comparative Study of High-Cycle Fatigue and Failure Mechanisms in Ultrahigh-Strength CrNiMoWMnV Low-Alloy Steels
- 2024Microstructure Characterization and Mechanical Properties of Polymer‐Derived (Hf<sub><i>x</i></sub>Ta<sub>1−<i>x</i></sub>)C/SiC Ceramic Prepared upon Field‐Assisted Sintering Technique/Spark Plasma Sinteringcitations
- 2024Dealing with Missing Angular Sections in NanoCT Reconstructions of Low Contrast Polymeric Samples Employing a Mechanical In Situ Loading Stage
- 2024The effect of grain boundaries and precipitates on the mechanical behavior of the refractory compositionally complex alloy NbMoCrTiAlcitations
- 2023Dealing with missing angular sections in nanoCT reconstructions of low contrast polymeric samples employing a mechanical in situ loading stage
- 20233D‐Printed Inherently Porous Structures with Tetrahedral Lattice Architecture: Experimental and Computational Study of Their Mechanical Behavior
- 2022Lab-based in situ nanoCT as a tool for the 3D structural and mechanical characterization of metamaterials
- 2021Architectural tunability of mechanical metamaterials in the nanometer rangecitations
- 2021Controlling shear band instability by nanoscale heterogeneities in metallic nanoglassescitations
- 2021Optimization of sintering conditions for improved microstructural and mechanical properties of dense Ce0.8Gd0.2O2-δ-FeCo2O4 oxygen transport membranescitations
- 2020Dislocation structures and the role of grain boundaries in cyclically deformed Ni micropillarscitations
- 2020Nanoscale patterning at the Si/SiO<sub>2</sub>/graphene interface by focused He<sup>+</sup> beamcitations
- 2019Size Effect on the Strength and Deformation Behavior of Glassy Carbon Nanopillars
- 2019Sliding wear behavior of fully nanotwinned Cu alloys
- 2018Micromechanics-based investigation of the elastic properties of polymer-modified cementitious materials using nanoindentation and semi-analytical modelingcitations
- 2017Annealing-induced recovery of indents in thin Au(Fe) bilayer films
- 2017Micromechanical study on the deformation behavior of directionally solidified NiAl–Cr eutectic compositescitations
- 2017Micromechanics-based prediction of the elastic properties of polymer-modified cementitious materials
- 2016Hydration of magnesia cubes: a helium ion microscopy study
- 2016Deformation mechanisms and morphology of metallic multilayers revealed by nanosliding and nanoindentation
- 2006Size effects on deformation and fracture of nanostructured metalscitations
Places of action
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article
Microstructure Characterization and Mechanical Properties of Polymer‐Derived (Hf<sub><i>x</i></sub>Ta<sub>1−<i>x</i></sub>)C/SiC Ceramic Prepared upon Field‐Assisted Sintering Technique/Spark Plasma Sintering
Abstract
<jats:p>The high‐temperature microstructural evolution and mechanical properties of two SiC‐based polymer‐derived ceramics with different Hf:Ta molar ratios are investigated using electron microscopy techniques and manipulated by nanoindentation. The as‐pyrolyzed ceramic powder consists of an amorphous Si(Hf<jats:sub><jats:italic>x</jats:italic></jats:sub>Ta<jats:sub>1−<jats:italic>x</jats:italic></jats:sub>)C(N,O) structure (where <jats:italic>x</jats:italic> = 0.2, 0.7) with localized nanocrystalline transition metal carbides (TMCs). Subsequent application of the field‐assisted sintering technique (FAST) for high‐temperature consolidation results in a crystalline (Hf<jats:sub><jats:italic>x</jats:italic></jats:sub>Ta<jats:sub>1−<jats:italic>x</jats:italic></jats:sub>)C/SiC ultra‐high temperature ceramic nanocomposite. The microstructure contains powder particle‐sized grains and sinter necks between the former powder particles. The powder particles consist of a β‐SiC matrix and small TMCs. Large TMCs are observed on the internal surfaces of former powder particles. This is due to the pulsed direct current and the resulting Joule heating that facilitates diffusion as well as oxygen impurities. Sinter necks of large β‐SiC grains form during the FAST process. The microstructural regions are assessed using high‐throughput nanoindentation. The hardness for SiC/(Hf<jats:sub>0.7</jats:sub>Ta<jats:sub>0.3</jats:sub>)C is measured on the formed grains and the sinter necks giving mean hardness values of about 27 and 37 GPa, respectively.</jats:p>